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1 article(s) from Suchsland, Ruth

Preparation of trinucleotide phosphoramidites as synthons for the synthesis of gene libraries

Ruth Suchsland,
Bettina Appel and
Sabine Müller

Beilstein J. Org. Chem. 2018, 14, 397–406, doi:10.3762/bjoc.14.28

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Graphical Abstract

Figure 1: Preparation of fully protected trinucleotides in solution (A), on solid phase (B) and on soluble po...

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Figure 2: Strategies for trinucleotide synthesis using different pairs of orthogonal groups for protection of...

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Figure 3: Strategy for the synthesis of nucleotide dimers and extension to the trimer in either 5'- or 3'-dir...

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Figure 4: Removal of the 3'-O-protecting group under conditions that leave all other protecting groups at 5'-...

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Figure 5: Release of trinucleotide blocks from the solid support by cleavage of an oxalyl anchor (A) and by a...

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Figure 6: Release of the trinucleotide from the support under reductive conditions.

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Figure 7: Phosphitylation of trimers. Reaction conditions, in particular the choice of the phosphitylation re...

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Review

Published 13 Feb 2018

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